Notes: Green 0-2% Acceptable Orange % Alert Red 3.1 and up Fail. Calibrated By:

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Metco MultiCoat Certificate of Calibration Cert. No. : 2008-036 Page: 1 of 10 Customer: ABC Console Metco MultiCoat Feeder: Metco 9MPE-DJ-CL Address: 6732 8 St. NE S/N: SM044588 Serial Number: A9MPEDJCL20080708-1 City: Calgary Device ID#: HTI 00-033 Device ID: HTI 00-058 State/Province: Albert, Canada Booth #: 1 Zip: T2E 7H7 With in 3%: No Feeder: Metco 9MPE-CL Name: St Charles Adjustments: Yes Serial Number: A9MPCL20010525-1 Phone #: 403-221-1410 Device ID: HTI 00-057 N.I.S.T. Instruments Used for This Calibration Test Inst: Press. Transducer Test Inst: Multi Meter Test Inst: Amp Clamp Test Inst: Make: Fluke Make: Fluke Make: Fluke Make: Model: PV350 Model: 87V Model: i1010 Model: Serial No: 107 Serial No: 88190113 Serial No: 91562357 Serial #: Next Cal. Due: 1/11/2009 Next Cal. Due: 7/31/2008 Next Cal. Due: 3/11/2009 Next Cal. Due: Test Inst: Low Flow Mass Flow Meter Test Inst: Med. Flow Mass Flow Meter Test Inst: High Flow Mass Flow Meter Make: Bronkhorst 0-75 scfh Make: Bronkhorst 0-400 Scfh Make: Bronkhorst 0-2500 Scfh Model: FM21-RBA-22-V Model: FM31-RBA-55-V Model: F-113Al-RBA-55-V Serial No: M5202125C Serial No: M5202125B Serial No: M5202125D Next Cal. Due: 12/21/2008 Next Cal. Due: 12/21/2008 Next Cal. Due: 12/26/2008 Plasma Plasma Plasma Plasma HVOF HVOF HVOF HVOF Mass Flow Controller: Argon Primary Nitrogen Primary Hydrogen Helium Oxygen Hydrogen Methane Air Make: Bronkhorst Bronkhorst Bronkhorst Bronkhorst Bronkhorst Bronkhorst Bronkhorst Bronkhorst Device ID: HTI 00-034 HTI 00-035 HTI 00-036 HTI 00-037 HTI 00-103 HTI 00-104 HTI 00-105 HTI 00-102 Serial Number: M4205992E M2202053AZ M4205594L M4205992V M4100848A M4203899H M4201257B M4204007E Flow Range: 100 ln/min 100 ln/min 20 ln/min 200 ln/min 400 ln/min 800 ln/min xxxx 800 ln/min Notes: System Performance w/prameters as Provided by the Operator Initially Evidence of Gas Contamination Gas SCFH Setting Gun Gas SCFH Setting Gun Oxygen Oxygen 635 DJ 2700 Argon F4 Hydrogen (H2) Hydrogen (H2) N/A Hydrogen Volts Propylene (C3H6) Propylene (C3H6) N/A Nitrogen Propane (C3H8) Propane (C3H8) N/A Amps Shroud Air Shroud Air 630 Natural Gas (CH4) Natural Gas (CH4) 431 Calibrated By: Allen Hildebrand Green 0-2% Acceptable Orange 2.1-3.0% Alert Red 3.1 and up Fail

Customer: ABC Oxygen Flow Cert. No: 2008-036 Page: 2 of 10 Console: Metco MultiCoat Serial Number: SM044588 Type of Gas: Oxygen Full Flow SCFH [FS]: 914 Device ID #: HTI 00-103 Booth: 1 Scale Rate: Flow is in SCFH Device Under Test: O2 Mass Flow Contrl. Make: Bronkhorst Serial Number: M4100848A Flow Range: 400 ln/min Testing Instrument: Mass Flow Meter Bronkhorst 0-2500 Scfh Serial Number: M5202125D Test Inst. Multi Meter 87V Serial Number: 88190113 Metco MultiCoat Metco MultiCoat As Found As Found As Found Actual As Found SCFH As Left As Left As Left As Left SCFH % Previous Display Actual SCFH Set Point NIST Volts SCFH Actual SCFH Deviation % Deviation NIST Volts Actual SCFH SCFH Deviation Deviation SCFH 200 200 0.828 204.5 4.5 0.5 0.852 210.4 10.4 1.1 300 300 1.210 298.9-1.1-0.1 1.244 307.3 7.3 0.8 400 400 1.584 391.2-8.8-1.0 1.630 402.6 2.6 0.3 500 500 1.948 481.2-18.8-2.1 2.016 498.0-2.0-0.2 600 600 2.318 572.5-27.5-3.0 2.409 595.0-5.0-0.5 699 700 2.683 662.7-37.3-4.1 2.805 692.8-7.2-0.8 800 800 3.061 756.1-43.9-4.8 3.212 793.4-6.6-0.7 899 900 3.450 852.2-47.9-5.2 3.629 896.4-3.6-0.4 100 90 80 70 60 50 40 30 20 10 1 2 3 4 5 6 7 8 Flow SCFH As Found 204.5 298.9 391.2 481.2 572.5 662.7 756.1 852.2 Flow SCFH As Left 210.4 307.3 402.6 498.0 595.0 692.8 793.4 896.4 Set Point SCFH 200 300 400 500 600 700 800 900

Customer: ABC Air Flow Cert. No: 2008-036 Page: 3 of 10 Console: Metco MultiCoat Serial Number: SM044588 Type of Gas: Air Full Flow SCFH [FS]: 1827 Device ID #: HTI 00-102 Booth: 1 Scale Rate: Flow is in SCFH Device Under Test: Air Mass Flow Contr. Make: Bronkhorst Serial Number: M4204007E Flow Range: 800 ln/min Testing Instrument: Mass Flow Meter Bronkhorst 0-2500 Scfh Serial Number: M5202125D Test Inst. Multi Meter 87V Serial Number: 88190113 Metco MultiCoat Metco MultiCoat As Found As Found As Found Actual As Found SCFH As Left As Left As Left As Left SCFH % Previous Display Actual SCFH Set Point NIST Volts SCFH Actual SCFH Deviation % Deviation NIST Volts Actual SCFH SCFH Deviation Deviation SCFH 350 350 1.313 328.3-21.8-1.0 1.420 355.0 5.0 0.2 650 650 2.427 606.8-43.3-1.9 2.606 651.5 1.5 0.1 950 950 3.506 876.5-73.5-3.3 3.771 942.8-7.3-0.3 1250 1250 4.480 112-13 -5.9 4.959 1239.8-10.3-0.5 1550 1550 5.682 1420.5-129.5-5.8 6.200 155 180 160 140 120 100 80 60 40 20 1 2 3 4 5 Flow SCFH As Found 328.3 606.8 876.5 112 1420.5 Flow SCFH As Left 355.0 651.5 942.8 1239.8 155 Set Point SCFH 350 650 950 1250 1550

Calibration Not Required, Not Used for Parameters Customer: ABC Hydrogen Flow Cert. No: 2008-036 Page: 4 of 10 Console: DJC Serial Number: SM044588 Type of Gas: Hydrogen Full Flow SCFH [FS]: 1827 Device ID #: HTI 00-104 Booth: 1 Scale Rate: Flow is in SCFH Device Under Test: H2 Mass Flow Contr. Make: Bronkhorst Serial Number: M4203899H Flow Range: 20 ln/min Testing Instrument: Mass Flow Meter Bronkhorst 0-2500 Scfh Serial Number: M5202125D Test Inst. Multi Meter 87V Serial Number: 88190113 Metco MultiCoat Metco MultiCoat As Found As Found As Found Actual As Found SCFH As Left As Left As Left As Left SCFH % Previous Display Actual SCFH Set Point NIST Volts SCFH Actual SCFH Deviation % Deviation NIST Volts Actual SCFH SCFH Deviation Deviation SCFH 200 400 600 800 1000 1200 1400 1600 1800 200 180 160 140 120 100 80 60 40 20 1 2 3 4 5 6 7 8 9 Flow SCFH As Found Flow SCFH As Left Set Point SCFH 200 400 600 800 1000 1200 1400 1600 1800

Customer: ABC Methane Gas Flow Cert. No: 2008-036 Page: 5 of 10 Console: Metco MultiCoat Serial Number: SM044588 Type of Gas: Methane Full Flow SCFH [FS]: 570 Device ID #: HTI 00-105 Booth: 1 Scale Rate: Flow is in SCFH Device Under Test: C2H4 Mass Flow Cnt. Make: Bronkhorst Serial Number: M4201257B Flow Range: xxxx Testing Instrument: Mass Flow Meter Bronkhorst 0-2500 Scfh Serial Number: M5202125D Test Inst. Multi Meter 87V Serial Number: 88190113 Metco MultiCoat Metco MultiCoat As Found As Found As Found Actual As Found SCFH As Left As Left As Left As Left SCFH % Previous Display Actual SCFH Set Point NIST Volts SCFH Actual SCFH Deviation % Deviation NIST Volts Actual SCFH SCFH Deviation Deviation SCFH 50 50 0.204 38.8-11.2-2.0 0.252 47.9-2.1-0.4 150 150 0.702 133.4-16.6-2.9 0.808 153.5 3.5 0.6 250 250 1.176 223.4-26.6-4.7 1.309 248.7-1.3-0.2 350 350 1.634 310.5-39.5-6.9 1.846 350.7 0.7 0.1 450 450 2.100 399.0-51.0-8.9 2.355 447.5-2.6-0.4 550 550 2.569 488.1-61.9-10.9 2.900 551.0 1.0 0.2 60 50 40 30 20 10 1 2 3 4 5 6 Flow SCFH As Found 38.8 133.4 223.4 310.5 399.0 488.1 Flow SCFH As Left 47.9 153.5 248.7 350.7 447.5 551.0 Set Point SCFH 50 150 250 350 450 550

Customer: ABC Argon Flow Cert. No: 2008-036 Page: 6 of 10 Console: Metco MultiCoat Serial Number: SM044588 Type of Gas: Argon Full Flow SCFH [FS]: 228.3 Device ID #: HTI 00-034 Booth: 1 Scale Rate: Flow is in SCFH Device Under Test: Ar Mass Flow Contr. Make: Bronkhorst Serial Number: M4205992E Flow Range: 100 ln/min Testing Instrument: Mass Flow Meter Bronkhorst 0-400 Scfh Serial Number: 107020333384001 Testing Instrument: Multi Meter 87V Serial Number: 88190113 Metco MultiCoat Metco MultiCoat As Found As Found As Found Actual As Found SCFH As Left As Left As Left As Left SCFH Previous Display Actual SCFH Set Point NIST Volts Actual SCFH SCFH Deviation % Deviation NIST Volts Actual SCFH SCFH Deviation % Deviation SCFH 30 30 0.510 28.6-1.4-0.6 0.537 30.1 0.1 60 60 1.045 58.5-1.5-0.6 1.095 61.3 1.3 0.6 90 90 1.550 86.8-3.2-1.4 1.620 90.7 0.7 0.3 120 120 2.040 114.2-5.8-2.5 2.135 119.6-0.4-0.2 150 150 2.530 141.7-8.3-3.6 2.660 149.0-1.0-0.5 180 180 3.030 169.7-10.3-4.5 3.200 179.2-0.8-0.4 210 210 3.545 198.5-11.5-5.0 3.760 210.6 0.6 0.2 25 20 15 10 5 1 2 3 4 5 6 7 Flow SCFH As Found 28.6 58.5 86.8 114.2 141.7 169.7 198.5 Flow SCFH As Left 30.1 61.3 90.7 119.6 149.0 179.2 210.6 SCFH Target Values 30 60 90 120 150 180 210

Customer: ABC Nitrogen Flow Cert. No: 2008-036 Page: 7 of 10 Console: Metco MultiCoat Serial Number: SM044588 Type of Gas: Nitrogen Full Flow SCFH [FS]: 228.3 Device ID #: HTI 00-035 Booth: 1 Scale Rate: Flow is in SCFH Device Under Test: N2 Mass Flow Contrl. Make: Bronkhorst Serial Number: M2202053AZ Flow Range: 100 ln/min Testing Instrument: Mass Flow Meter Bronkhorst 0-400 Scfh Serial Number: 107020333384001 Testing Instrument: Multi Meter 87V Serial Number: 88190113 Metco MultiCoat Metco MultiCoat As Found As Found As Found Actual As Found SCFH As Left As Left As Left As Left SCFH Previous Display Actual SCFH Set Point NIST Volts Actual SCFH SCFH Deviation % Deviation NIST Volts Actual SCFH SCFH Deviation % Deviation SCFH 30 30 0.715 28.6-1.4-0.6 0.750 3 60 60 1.440 57.6-2.4-1.1 1.510 60.4 0.4 0.2 90 90 2.130 85.2-4.8-2.1 2.240 89.6-0.4-0.2 120 120 2.810 112.4-7.6-3.3 2.963 118.5-1.5-0.6 150 150 3.500 14-1 -4.4 3.710 148.4-1.6-0.7 180 180 4.201 168.0-12.0-5.2 4.465 178.6-1.4-0.6 210 210 4.916 196.6-13.4-5.9 5.257 210.3 0.3 0.1 25 20 15 10 5 1 2 3 4 5 6 7 Flow SCFH As Found 28.6 57.6 85.2 112.4 14 168.0 196.6 Flow SCFH As Left 3 60.4 89.6 118.5 148.4 178.6 210.3 SCFH Target Values 30 60 90 120 150 180 210

Customer: ABC Helium Flow Cert. No: 2008-036 Page: 8 of 10 Console: Metco MultiCoat Serial Number: SM044588 Type of Gas: Helium Full Flow SCFH [FS]: 457 Device ID #: HTI 00-037 Booth: 1 Scale Rate: Flow is in SCFH Device Under Test: He Mass Flow Contr. Make: Bronkhorst Serial Number: M4205992V Flow Range: 200 ln/min Testing Instrument: Mass Flow Meter Bronkhorst 0-400 Scfh Serial Number: 107020333384001 Testing Instrument: Multi Meter 87V Serial Number: 88190113 Metco MultiCoat Metco MultiCoat As Found As Found As Found Actual As Found SCFH As Left As Left As Left As Left SCFH Previous Display Actual SCFH Set Point NIST Volts Actual SCFH SCFH Deviation % Deviation NIST Volts Actual SCFH SCFH Deviation % Deviation SCFH 50 50 0.918 51.8 1.8 0.4 0.918 51.8 1.8 0.4 100 100 1.830 103.2 3.2 0.7 1.830 103.2 3.2 0.7 151 150 2.700 152.3 2.3 0.5 2.700 152.3 2.3 0.5 200 200 3.562 200.9 0.9 0.2 3.562 200.9 0.9 0.2 251 250 4.414 248.9-1.1-0.2 4.414 248.9-1.1-0.2 301 300 5.292 298.5-1.5-0.3 5.292 298.5-1.5-0.3 351 350 6.200 349.7-0.3-0.1 6.200 349.7-0.3-0.1 401 400 7.140 402.7 2.7 0.6 7.140 402.7 2.7 0.6 450 450 8.150 459.7 9.7 2.1 8.150 459.7 9.7 2.1 50 45 40 35 30 25 20 15 10 5 1 2 3 4 5 6 7 8 9 Flow SCFH As Found 51.8 103.2 152.3 200.9 248.9 298.5 349.7 402.7 459.7 Flow SCFH As Left 51.8 103.2 152.3 200.9 248.9 298.5 349.7 402.7 459.7 SCFH Set Point 50 100 150 200 250 300 350 400 450

Customer: ABC Hydrogen Flow Cert. No: 2008-036 Page: 9 of 10 Console: Metco MultiCoat Serial Number: SM044588 Type of Gas: Hydrogen Full Flow SCFH [FS]: 45.7 Device ID #: HTI 00-036 Booth: 1 Scale Rate: Flow is in SCFH Device Under Test: H2 Mass Flow Contr. Make: Bronkhorst Serial Number: M4203899H Flow Range: 20 ln/min Testing Instrument: Mass Flow Meter Bronkhorst 0-75 scfh Serial Number: M5202125C Testing Instrument: Multi Meter 87V Serial Number: 88190113 Metco MultiCoat Metco MultiCoat As Found As Found As Found Actual As Found SCFH As Left As Left As Left As Left SCFH Previous Display Actual SCFH Set Point NIST Volts Actual SCFH SCFH Deviation % Deviation NIST Volts Actual SCFH SCFH Deviation % Deviation SCFH 5 5 0.650 4.9-0.1-0.2 0.650 4.9-0.1-0.2 10 10 1.320 1 1.320 1 15 15 1.973 14.9-0.1-0.1 1.973 14.9-0.1-0.1 20 20 2.624 19.9-0.1-0.3 2.624 19.9-0.1-0.3 25 25 3.280 24.8-0.2-0.3 3.280 24.8-0.2-0.3 30 30 3.950 29.9-0.1-0.2 3.950 29.9-0.1-0.2 35 35 4.645 35.2 0.2 0.4 4.645 35.2 0.2 0.4 40 40 5.380 40.8 0.8 1.6 5.380 40.8 0.8 1.6 45.0 4 35.0 3 25.0 2 15.0 1 5.0 1 2 3 4 5 6 7 8 Flow SCFH As Found 4.9 1 14.9 19.9 24.8 29.9 35.2 40.8 Flow SCFH As Left 4.9 1 14.9 19.9 24.8 29.9 35.2 40.8 SCFH Target Values 5 10 15 20 25 30 35 40

Customer: ABC Amperage and Voltage Meter Cert. No. : 2008-036 Page: 10 of 10 Console: Metco MultiCoat Serial Number: SM044588 Booth : 1 Device ID #: Testing Instrument: Amp Clamp i1010 Serial Number: 91562357 Testing Instrument: Multi Meter 87V Serial Number: 88190113 Amp Meter Device Under Test: Digital Amp Meter Amps Full Scale [FS] 2000 Amps Meter NIST Actual Amps % Amps As Left As Left Amps As Left Set Point Reading Meter Deviation Deviation Meter Reading Deviation % Amps Deviation 300 300 303.0 3.0 0.2 303.0 3.0 0.2 400 400 405.0 5.0 0.3 405.0 5.0 0.3 500 500 507.0 7.0 0.4 507.0 7.0 0.4 600 600 61 1 0.5 61 1 0.5 700 700 712.0 12.0 0.6 712.0 12.0 0.6 800 800 815.0 15.0 0.8 815.0 15.0 0.8 900 900 918.0 18.0 0.9 918.0 18.0 0.9 Volt Meter Device Under Test: Digital Volt Meter Volts Full Scale [FS] 200 Volt Meter Display NIST Volts % Volts Volts As Left As Left As Left Set Point Reading Meter Deviation Deviation Meter Reading Volts Deviation % Volts Deviation 33.9 33.9 34.5 0.6 0.3 34.5 0.6 0.3 34.5 34.5 34.1-0.4-0.2 34.1-0.4-0.2 53.4 52.4 53.0-0.4-0.2 61.9 8.5 4.3 57.2 57.2 57.7 0.5 0.3 57.7 0.5 0.3 61.3 61.3 61.9 0.6 0.3 53.0-8.3-4.2 Calibrated By: Allen Hildebrand